Atmospheric grinding was carried out in a planetary ball mill (P-7, Fritsch, Germany). Raw shells (5.0 g) and 60.0 g of 3.0 mm yttria-stabilized zirconia ball (Nikkato, Osaka, Japan) were placed into a zirconia pot with a volume of 45 cm 3 and a diameter of 39.95 mm. The revolution speed was adjusted to 400 rpm.
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